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Beilstein J. Org. Chem. 2021, 17, 2650–2656, doi:10.3762/bjoc.17.178
Graphical Abstract
Scheme 1: C(sp3)–H alkynylation of tetrahydroisoquinolines. L* = chiral ligand. TEMPO = 2,2,6,6-tetramethylpi...
Scheme 2: Substrate scope. Reaction conditions: Pt anode, Pt cathode, interelectrode distance 0.25 mm, 1 (0.0...
Scheme 3: Reaction scale-up.
Scheme 4: Proposed mechanism.